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CCR Mössbauer cryostat specifications

 CCS-800-205
Cooling typeCCR
Temperature range<5 K to 300 K1
Typical temperature stability2±50 mK
Sample environmentExchange gas
Optical
Sample chamber inner diameter38 mm (1.5 in)
Rotatable sample
Cooldown2.5 h
Cold head locationBottom
Typical vibrational line broadening0.01 mm/s
Height (approximate)142 to 168 cm (56 to 66 in)
Weight (approximate)27.2 kg (60 lb) cryostat and 327 kg (720 lb) stand (including lead shielding)
Window block size57.2 mm (2.25 in) OD
1Sample tube must be evacuated at temperatures above 150 K
2Measured with temperature controller

Facility requirements

Water-cooled

CCS-Cold headRecommended compressor maintenance intervalRecommended cold head maintenance interval60 Hz power requirements50 Hz power requirementsCooling water requirementsCompressor size
800-20530,000 h10,000 h200 VAC, 3-phase, 4.6 to 5.6 kW or 460 to 480 VAC, 3-phase, 4.6 to 5.6 kW200 VAC, 3-phase, 3.6 to 4.8 kW or 380/400/415 VAC, 3-phase, 3.6 to 4.8 kW4 to 9 L/min at 5 to 25 °C442 mm × 493 mm × 532 mm high; 96 kg

Air-cooled

CCS-Cold headRecommended compressor maintenance intervalRecommended cold head maintenance interval60 Hz power requirements50 Hz power requirementsCooling air requirementsCompressor size
800-20530,000 h10,000 h200 VAC, 3-phase, 4.6 to 6.4 kW or 460 to 480 VAC, 3-phase, 4.6 to 6.4 kW200 VAC, 3-phase, 3.6 to 5.4 kW or 380/400/415 VAC, 3-phase, 3.6 to 5.4 kW17.6 m3/min (60 Hz) or 14.7 m3/min (50 Hz) 442 mm × 493 mm × 889 mm high; 110 kg


CCS-850 mossbauer spectra chartShown to the right are Fe57 Mössbauer spectra (dots) of a 25 µm iron metal foil at 298 K with the CCR off and on. The velocity scan of ±2 mm/s covers only the innermost lines of the iron metal sextet. Also shown are least squares fits (lines) of a symmetric quadrupole pair with Lorentzian line shapes to each spectrum. The results of the fits were linewidth estimates of 0.234 mm/s with the CCR off and 0.241 mm/s with the CCR on. The uncertainty in the line width estimates due to the counting statistics is ±0.002 mm/s.

NOTE: Data provided by Science Engineering & Education Co. (SEE Co. — formerly Web Research Co.), http://www.seeco.us. Special thanks to Professor Darby Dyar, Mount Holyoke College.